A Facile Microwave-Assisted 'One-Pot' Synthesis of Piperazino Pyrimidinyl Acetamides, a Class of Hybrid Bis Heterocycles and Their Structural Elucidation Using NMR Spectral Techniques

Autor:	Ghee Ang How, Choon Ng Siu, V. Kanagarajan, Mannathusamy Gopalakrishnan
Rok vydání:	2013
Předmět:	Dry media reaction Elemental analysis Chemistry Organic Chemistry One-pot synthesis Microwave irradiation Melting point Organic chemistry Microwave assisted Combinatorial chemistry Heteronuclear single quantum coherence spectroscopy Catalysis
Zdroj:	Journal of Heterocyclic Chemistry. 50:396-402
ISSN:	0022-152X
DOI:	10.1002/jhet.1046
Popis:	An array of novel piperazino pyrimidinyl acetamides, a class of hybrid bis heterocycles are synthesized in “one-pot” by microwave irradiation method catalyzed by heterogeneous NaHSO4.SiO2 catalyst in dry media and are characterized by melting point, elemental analysis, MS, FT-IR, one-dimensional NMR (1H and 13C) and two-dimensional 1H-1H COSY and 1H-13C HSQC spectral data.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::2ea1644326c17e5a4661195e0e8838ed https://doi.org/10.1002/jhet.1046 Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
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