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The objective of this study was to determine the effects of different manufacturing processes of Galotyri-type cheese on its free fatty acid (FFA) profile and volatile compounds. Three cheesemaking methods were evaluated, namely production of cheese using salted ewes’ milk, starter culture and rennet (SM+R), and starter culture with or without rennet and salting the curd after draining (R+SC or SC, respectively). Lauric, palmitic and acetic were the most abundant FFA in all cheeses during storage. The SC+R cheese had significantly (P |