Effect of Synthesis Conditions on the Phase Composition and Structure of Nickel-Based Microspheres Prepared by Exothermic Synthesis from a Glycine–Nitrate Solution

Autor:	N. Yu. Melnik, K. B. Podbolotov, Aliaksandr Khort, A. A. Shegidevich
Rok vydání:	2020
Předmět:	010302 applied physics Exothermic reaction Materials science General Chemical Engineering Non-blocking I/O Metals and Alloys chemistry.chemical_element 02 engineering and technology 021001 nanoscience & nanotechnology 01 natural sciences Inorganic Chemistry Nickel chemistry.chemical_compound chemistry Nitrate Chemical engineering Phase composition 0103 physical sciences Glycine Materials Chemistry Composition (visual arts) Crystallite 0210 nano-technology
Zdroj:	Inorganic Materials. 56:473-481
ISSN:	1608-3172 0020-1685
DOI:	10.1134/s0020168520050118
Popis:	We report our findings on the influence of composition and reaction temperature on the phase composition and structure of nickel-based microspheres prepared by combining exothermic synthesis and spray pyrolysis from a glycine–nitrate solution. It has been shown that, at the optimal reductant-to-oxidant ratio and reaction temperature, the microspheres consist of Ni, Ni3N, and NiO, and the nickel content reaches 98%. The synthesized material has the form of microspheres 0.5 to 1.5 μm in average diameter and 10 to 15 nm in crystallite size.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::2abce758974a05b7d9560b74508e648e https://doi.org/10.1134/s0020168520050118 Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
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