Solid state synthesis and structural characterization of zinc titanates
| Autor: | Hamadi Khemakhem, Adel Matoussi, Sarra Ayed, Helmi Abdelkefi |
|---|---|
| Rok vydání: | 2016 |
| Předmět: |
Materials science
Inorganic chemistry Oxide Infrared spectroscopy chemistry.chemical_element 02 engineering and technology Zinc engineering.material 010402 general chemistry 01 natural sciences symbols.namesake chemistry.chemical_compound Materials Chemistry Wurtzite crystal structure Mechanical Engineering Spinel Metals and Alloys 021001 nanoscience & nanotechnology 0104 chemical sciences chemistry Chemical engineering Mechanics of Materials symbols engineering 0210 nano-technology Raman spectroscopy Zinc titanate Titanium |
| Zdroj: | Journal of Alloys and Compounds. 677:185-189 |
| ISSN: | 0925-8388 |
| DOI: | 10.1016/j.jallcom.2016.03.244 |
| Popis: | Zinc titanate composite materials were synthesized via solid state sintering process using high-purity metal oxide powders (purity ∼99.99%). The titanium incorporation into ZnO matrix was investigated by X-ray diffraction which revealed the coexistence of spinel Zn 2 TiO 4 and hexagonal ZnTiO 3 with the ZnO wurtzite structures. No reflection peaks of rutile TiO 2 phase were detected. The IR spectroscopy and Raman scattering spectroscopy were used to characterize the structural and chemical properties of the ZnO/TiO 2 composites. The IR bands and vibrational modes of all crystalline phases were detected. The effect of TiO 2 doping rates (x = 3, 5 and 7 wt%) on bands shifting, Raman intensity and structural quality was discussed. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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