Growth of platinum fibers using the micro-pulling-down method
Autor: | Yuji Ohashi, Mototaka Arakawa, Shunsuke Kurosawa, Yuui Yokota, Kei Kamada, Valery Chani, Akira Yoshikawa, Takayuki Nihei |
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Rok vydání: | 2017 |
Předmět: |
010302 applied physics
Materials science Scanning electron microscope chemistry.chemical_element Crucible Micro-pulling-down Crystal growth 02 engineering and technology 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences Inorganic Chemistry Crystallography chemistry visual_art 0103 physical sciences Materials Chemistry visual_art.visual_art_medium Grain boundary Fiber Ceramic Composite material 0210 nano-technology Platinum |
Zdroj: | Journal of Crystal Growth. 468:403-406 |
ISSN: | 0022-0248 |
DOI: | 10.1016/j.jcrysgro.2016.10.088 |
Popis: | Platinum (Pt) crystalline fibers were grown from the melt by the micro-pulling-down (μ-PD) method using the ZrO 2 ceramics crucible. The diameter of the grown Pt fiber was controlled by the ϕ1 mm outlet made at the bottom of the crucible and the Pt fiber of 0.95±0.03 mm in diameter and over 5 m in length was obtained at 10 mm/min pulling-down rate. In addition, the Pt fiber was grown at 1–110 mm/min pulling rates while the liquid-solid interface reached the bottom of the crucible and the crystal growth became unstable at 120 mm/min pulling rate. Few grain boundaries were observed in the scanning electron microscopy image of the Pt fibers and there were some spots with high intensity in the pole figures. |
Databáze: | OpenAIRE |
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