Effects of synthesis variables on the magnetic properties of CoFe2O4 nanoparticles
| Autor: | Werner Brämer-Escamilla, Gerzon E. Delgado, Sarah Briceño, Pedro Silva, Eric Plaza, Edgard Cañizales, Jordana Palacios |
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| Rok vydání: | 2012 |
| Předmět: |
Thermogravimetric analysis
Materials science Scanning electron microscope Annealing (metallurgy) Analytical chemistry Nanoparticle Coercivity Condensed Matter Physics Electronic Optical and Magnetic Materials Nuclear magnetic resonance Differential thermal analysis Fourier transform infrared spectroscopy High-resolution transmission electron microscopy human activities |
| Zdroj: | Journal of Magnetism and Magnetic Materials. 324:2926-2931 |
| ISSN: | 0304-8853 |
| DOI: | 10.1016/j.jmmm.2012.04.051 |
| Popis: | Cobalt ferrite nanoparticles (CoFe 2 O 4 ) have been synthesized using precipitation in water solution with polyethylene glycol as surfactant. Influence of various synthesis variables included pH, reaction time and annealing temperature on the magnetic properties and particle sizes has also been studied. Structural identification of the samples was carried out using Thermogravimetric and Differential thermal analysis, X-ray diffraction, Fourier transform infrared spectroscopy, Scanning electron microscopy, High resolution transmission electron microscopy. Vibrating sample magnetometer was used for the magnetic investigation of the samples. Magnetic properties of nanoparticles show strong dependence on the particle size. The magnetic properties increase with pH of the precipitating medium and annealing temperature while the coercivity goes through a maximum, peaking at around 25 nm. |
| Databáze: | OpenAIRE |
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