Formation and investigation of plasma nanostructured hafnia coatings

Autor: M. N. Polyansky, A. A. Ashmarin, S. V. Savushkina, E. A. Vysotina, G. V. Panasova, L. E. Agureev
Rok vydání: 2019
Předmět:
Zdroj: Journal of Physics: Conference Series. 1238:012035
ISSN: 1742-6596
1742-6588
DOI: 10.1088/1742-6596/1238/1/012035
Popis: Nanostructured coatings HfO2-9wt%Y2O3 were obtained by plasma spraying in vacuum using supersonic nozzle creating Prandtl-Mayer expansion fan. The coatings were investigated by scanning electron microscopy, X-ray diffraction analysis, and synchronous thermal analysis (differential scanning calorimetry, thermogravimetric analysis, and differential thermogravimetric analysis) in the temperature range of 40÷1600°C. The coatings are predominantly characterized by the nanostructured globular structure. Thermal analysis showed a peak corresponding to the exothermic reaction in the temperature range of 1400÷1600 °C, accompanied by a mass loss. c-HfO2 phase remained in the coating after thermal analysis with a decrease in the lattice parameter a from 5.18 Å to 5.13 Å.
Databáze: OpenAIRE