Formation and investigation of plasma nanostructured hafnia coatings
Autor: | M. N. Polyansky, A. A. Ashmarin, S. V. Savushkina, E. A. Vysotina, G. V. Panasova, L. E. Agureev |
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Rok vydání: | 2019 |
Předmět: | |
Zdroj: | Journal of Physics: Conference Series. 1238:012035 |
ISSN: | 1742-6596 1742-6588 |
DOI: | 10.1088/1742-6596/1238/1/012035 |
Popis: | Nanostructured coatings HfO2-9wt%Y2O3 were obtained by plasma spraying in vacuum using supersonic nozzle creating Prandtl-Mayer expansion fan. The coatings were investigated by scanning electron microscopy, X-ray diffraction analysis, and synchronous thermal analysis (differential scanning calorimetry, thermogravimetric analysis, and differential thermogravimetric analysis) in the temperature range of 40÷1600°C. The coatings are predominantly characterized by the nanostructured globular structure. Thermal analysis showed a peak corresponding to the exothermic reaction in the temperature range of 1400÷1600 °C, accompanied by a mass loss. c-HfO2 phase remained in the coating after thermal analysis with a decrease in the lattice parameter a from 5.18 Å to 5.13 Å. |
Databáze: | OpenAIRE |
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