Modification of Bethge's Open-System Apparatus for the Determination of Mercury in Biological Materials

Autor: O. O. Odukoya
Rok vydání: 1990
Předmět:
Zdroj: International Journal of Environmental Analytical Chemistry. 39:323-327
ISSN: 1029-0397
0306-7319
Popis: The performance of the open system (Bethge's apparatus) of digestion of biological materials for mercury analysis has been upgraded to compare favourably with the closed systems. Losses at the joints and during refluxing were successfully eliminated by the following modifications: (i) thin PTFE cylinders were used in the joints; (ii) a PTFE two-way stopper was used instead of the glass stopper in the original apparatus; (iii) a double-faced spiral condenser was used to increase the cooling efficiency and minimise losses.
Databáze: OpenAIRE