A method for the preparation of [13C6]-labelled 2-substituted naphthalenes

Autor:	George J. Ellames, John M. Herbert
Rok vydání:	2010
Předmět:	Annulation Chemistry Organic Chemistry Carbon-13 Reaction intermediate Biochemistry Chemical synthesis Analytical Chemistry chemistry.chemical_compound Isotopes of carbon Bromide Drug Discovery Organic chemistry Radiology Nuclear Medicine and imaging Xaliproden Spectroscopy Naphthalene
Zdroj:	Journal of Labelled Compounds and Radiopharmaceuticals. 53:801-803
ISSN:	0362-4803
DOI:	10.1002/jlcr.1798
Popis:	A reliable route is described for the preparation of various 2-substituted derivatives of [1,2,3,4,4a,8a-13C6]-naphthalene via the bromide 10. The approach is used to prepare [naphthalene-1,2,3,4,4a,8a-13C6]-2-(2-bromoethyl)naphthalene (1), a key intermediate in the synthesis of labelled SR57746A, Xaliproden (2). Copyright © 2010 John Wiley & Sons, Ltd.
Databáze:	OpenAIRE
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