Spectral, NLO, thermal, hardness and SEM studies of phosphate doped bis-urea oxalic acid crystals for laser applications

Autor:	S. Vasumathi, P Selvarajan, H Johnson Jeyakumar
Rok vydání:	2021
Předmět:	Crystal chemistry.chemical_compound Materials science chemistry Vickers hardness test Oxalic acid Doping Analytical chemistry General Physics and Astronomy Fourier transform infrared spectroscopy Evaporation (deposition) Single crystal Monoclinic crystal system
Zdroj:	Chinese Journal of Physics. 73:1-12
ISSN:	0577-9073
DOI:	10.1016/j.cjph.2021.06.008
Popis:	Phosphate doped bis-urea oxalic acid (PBUO) crystals were grown using the aqueous solution by slow evaporation technique. Single crystal XRD study indicates that the sample crystallizes in monoclinic structure. The mechanical parameters like hardness, yield strength and stiffness constant of the crystal were determined by using the Vickers hardness tester. UV-visible spectral studies were done to determine the various linear optical parameters. Second harmonic generation (SHG) efficiency was measured for the grown crystal of PBUO to understand the nonlinear optical activity. TG/DTA analysis shows that the PBUO crystal is thermally stable upto 170 °C. Energy dispersive X-ray analysis (EDAX) was carried out by recording the EDAX spectrum of the grown crystal to identify elements in the sample. The grown PBUO crystals were also characterized by FTIR, SEM, PL, LDT and impedance studies.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::244405ef6d6dd02cecb300aa698e3c5d https://doi.org/10.1016/j.cjph.2021.06.008 Zobrazit plný text záznamu Full Text from ScienceDirect