1,4-Cyclohexadiene with Pd/C as a rapid, safe transfer hydrogenation system with microwave heating
Autor: | Brian T. Gregg, John F. Quinn, Kathryn C. Golden, Dana A. Razzano |
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Rok vydání: | 2008 |
Předmět: | |
Zdroj: | Tetrahedron Letters. 49:6137-6140 |
ISSN: | 0040-4039 |
Popis: | A method for the rapid, safe hydrogenation of alkenes and deprotection of benzyl ethers and carboxybenzyl amides is described using catalytic transfer hydrogenation under microwave heating conditions. Commonly available Pd/C catalyst is extremely effective with 1,4-cyclohexadiene as the hydrogen transfer source. In general, the reactions are complete within five minutes at 100 °C. |
Databáze: | OpenAIRE |
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