Role of Mn+2 ions in monitoring structural, optical, magnetic and electrical properties of manganese zinc ferrite nanoparticles
| Autor: | Satish H.P. Keluskar, Pranav P. Naik, Vikas Pissurlekar, Snehal S. Hasolkar |
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| Rok vydání: | 2021 |
| Předmět: |
010302 applied physics
Materials science Scanning electron microscope Analytical chemistry chemistry.chemical_element Manganese Dielectric Condensed Matter Physics 01 natural sciences Atomic and Molecular Physics and Optics Nanocrystalline material Electronic Optical and Magnetic Materials Lattice constant chemistry Transmission electron microscopy 0103 physical sciences Ferrite (magnet) Electrical and Electronic Engineering Fourier transform infrared spectroscopy |
| Zdroj: | Journal of Materials Science: Materials in Electronics. 32:25840-25851 |
| ISSN: | 1573-482X 0957-4522 |
| DOI: | 10.1007/s10854-020-04945-9 |
| Popis: | Nanocrystalline manganese zinc ferrite powders with chemical composition MnxZn1−xFe2O4 were prepared using the combustion method. The X-ray diffraction (XRD) technique was used to confirm the phase formation. Structural parameters such as lattice constant and density showed appreciable dependence on varying manganese concentrations in the ferrite material. The structural bond analysis was achieved using Fourier transform infrared (FTIR) spectroscopy. The surface morphology of nanopowders was analyzed using a scanning electron microscope (SEM). The particle size estimation was done using a transmission electron microscope (TEM) and was found to be in the narrow range of 15–25 nm. The dependence of saturation magnetization on manganese concentration was investigated using a vibrating sample magnetometer (VSM). The variation of electrical properties such as dielectric constant and dielectric loss was also studied and were seen to be administered by cationic distribution at the tetrahedral and the octahedral sites in the spinel structure. |
| Databáze: | OpenAIRE |
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