| Autor: |
Xiao Jing Zhao, Li Ying Zhang, Li Ming Jim, Sheng Di Fan |
| Rok vydání: |
2013 |
| Předmět: |
|
| Zdroj: |
Applied Mechanics and Materials. 404:118-121 |
| ISSN: |
1662-7482 |
| DOI: |
10.4028/www.scientific.net/amm.404.118 |
| Popis: |
In the current paper, improvements were made to the synthesis of the peptide lipid N+C5Gly2C16 by recrystallization, which eliminated to need to use column chromatography for product purification in each step of the reaction. A simpler and more efficient synthesis process was obtained and every step of the reaction was improved. In particular steps 2 and 3 became closely associated, with the product of step 2 taken as the reactant of step 3 without purification to boost synthesis efficiency. A total synthesis ratio of 23% N+C5Gly2C16 was achieved from the synthesis. |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
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