Statistical student’s t-test in carbon nanospheres synthesis from cis-1,4-polyisoprene
| Autor: | Luis Zamora-Peredo, Francisco Gabriel Granados-Martínez, Leandro García-González, Diana Litzajaya García-Ruiz, Orlando Hernández-Cristóbal, Jaime A. Guzmán-Fuentes, Lada G. Domratcheva-Lvova, Yesenia Arredondo-León, Carmen Judith Gutiérrez-García, José de Jesús Contreras-Navarrete, Jael Madaí Ambriz-Torres, Erasmo Cadenas-Calderón |
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| Rok vydání: | 2020 |
| Předmět: |
Materials science
Mechanical Engineering Analytical chemistry chemistry.chemical_element 02 engineering and technology Chemical vapor deposition 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics Steel bar 01 natural sciences 0104 chemical sciences Catalysis symbols.namesake chemistry Mechanics of Materials symbols General Materials Science Tube (fluid conveyance) Fourier transform infrared spectroscopy 0210 nano-technology Raman spectroscopy Quartz Carbon |
| Zdroj: | MRS Advances. 5:3371-3377 |
| ISSN: | 2059-8521 |
| DOI: | 10.1557/adv.2020.399 |
| Popis: | A student’s t-test was applied in carbon nanospheres synthesis from cis-1,4-polyisoprene considering the green chemical principles. The synthesis was carried out by Chemical Vapor Deposition method with a quartz tube reactor using an AISI 304 steel bar as catalyst. It was possible to obtain two types of different samples, one from the surface of the steel bar (catalyst) and another from the quartz tube surface (without catalyst) in the same experiment. Carbon spheres were observed in both samples by micrographs obtained by FESEM. The Raman and FTIR spectroscopies shown characteristic bands of this carbon structures (G and D). The results obtained by student’s t-test proved a statistical significance between spheres means of samples collected from steel bar and quartz tube surface. |
| Databáze: | OpenAIRE |
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