Effect of silane compounds on bonding to fused quartz of tri-n-butylborane initiated resin
Autor: | Hiroyasu Koizumi, Hideo Matsumura, Akihisa Kodaira, Hiroshi Nogawa, Tomoyo Okazaki, Tomotaro Nihei |
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Rok vydání: | 2018 |
Předmět: |
Fused quartz
Materials science Bond strength Silicon dioxide 0206 medical engineering Tri-n-butylborane 030206 dentistry 02 engineering and technology Methacrylate 020601 biomedical engineering Silane law.invention 03 medical and health sciences chemistry.chemical_compound 0302 clinical medicine chemistry law Ceramics and Composites Methyl methacrylate General Dentistry Quartz Nuclear chemistry |
Zdroj: | Dental Materials Journal. 37:429-436 |
ISSN: | 1881-1361 0287-4547 |
DOI: | 10.4012/dmj.2017-183 |
Popis: | This study aimed to investigate how different compositions of experimental silane-based primers in a methyl methacrylate solution containing 3-(trimethoxysilyl)propyl methacrylate (3-TMSPMA) or 3-(4-methacryloyloxyphenyl)propyl trimethoxysilane (3-MPPTS) might act as silicon dioxide bonding agents. With or without post-silanization heat treatment, primer-treated quartz discs were bonded using the MMA-TBB resin and their bond strengths were evaluated. The disks were primed with one of the following materials: 1 mol% 3-TMSPMA, 2 mol% 3-TMSPMA, 1 mol% 3-MPPTS, and 2 mol% 3-MPPTS. Shear bond strength was determined both before and after thermocycling. Statistical analyses were performed with non-parametric procedure (Kruskal-Wallis, Mann-Whitney U, and Steel-Dwass tests). Both primers were effective with heat treatment to enhance bonding between quartz and the MMA-TBB, and the bonding durability of the 1 and 2 mol% 3-MPPTS (16.8 and 24.9 MPa) with heat groups was significantly higher than in the 1 and 2 mol% 3-TMSPMA (5.4 and 9.8 MPa) with heat groups. |
Databáze: | OpenAIRE |
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