Optimization of parameters through Taguchi method for enhanced corrosion inhibition of poly (vinyl alcohol-serine)
| Autor: | A. Ali Fathima Sabirneeza, A. Shahul Hameed, S. Subhashini |
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| Rok vydání: | 2015 |
| Předmět: |
Vinyl alcohol
Materials science Surfaces and Interfaces General Chemistry Polyvinyl alcohol Surfaces Coatings and Films Corrosion Thermogravimetry chemistry.chemical_compound Taguchi methods Differential scanning calorimetry chemistry Chemical engineering Mechanics of Materials Differential thermal analysis Materials Chemistry Composite material Fourier transform infrared spectroscopy |
| Zdroj: | Journal of Adhesion Science and Technology. 29:2648-2678 |
| ISSN: | 1568-5616 0169-4243 |
| DOI: | 10.1080/01694243.2015.1078922 |
| Popis: | Parametric optimization was carried out for the mixture of polyvinyl alcohol (PVA) and l-serine using Taguchi statistical approach. L9 orthogonal array of experiments were designed and the results were analyzed with Qualitek software. Synergistic effect of the mixture was enhanced at the Qualitek predicted optimized conditions. The graft polymer, poly(vinyl alcohol-serine) (PVAS), was synthesized using free radical-initiated reactions of l-serine with PVA in order to achieve effective inhibition. PVAS was characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, and powder X-ray diffraction analysis. The thermal properties of PVAS were studied by thermogravimetry, differential thermal analysis, and differential scanning calorimetry. The corrosion inhibition property of PVAS on mild steel corrosion was continuously monitored using electrochemical techniques. Temperature effect on the inhibition properties of PVAS was studied using electrochemical and gravimetric measurement... |
| Databáze: | OpenAIRE |
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