A Practical Gram-Scale Synthesis of Acrylohydroxamic Acid

Autor:	Bruce C. Hamper, Brendan T. Sullivan, Nigam P. Rath, Christopher D. Spilling
Rok vydání:	2017
Předmět:	010405 organic chemistry Organic Chemistry 010402 general chemistry Cleavage (embryo) 01 natural sciences Catalysis 0104 chemical sciences chemistry.chemical_compound Hydroxylamine Monomer chemistry Organic chemistry Chelation Amine gas treating Protecting group Acrylic acid Gram
Zdroj:	Synthesis. 49:5335-5338
ISSN:	1437-210X 0039-7881
DOI:	10.1055/s-0036-1589103
Popis:	Acrylohydroxamic acid, which is a useful monomer for the preparation of polymeric materials, has been prepared in a straightforward, two-step synthesis from readily available starting materials. The key steps are coupling of acrylic acid with O-tetrahydropyranylhydroxyl amine to provide protection of the hydroxylamine functionality, followed by acid cleavage of the protecting group.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::203d72e742d607069e7ffb025cb4685d https://doi.org/10.1055/s-0036-1589103 Zobrazit plný text záznamu