Crystal and Molecular Structure of Bi-1,1′-(3,3-dimethyl-3,4-dihydroisoquinoline)
Autor: | N. Yu. Merkur'eva, V. S. Sergienko, Yu. V. Shklyaev, Valentina I. Sokol, V. V. Davydov, Vladimir A. Glushkov |
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Rok vydání: | 2004 |
Předmět: | |
Zdroj: | Russian Journal of Coordination Chemistry. 30:144-149 |
ISSN: | 1070-3284 |
DOI: | 10.1023/b:ruco.0000015087.87685.29 |
Popis: | Bi-1,1′-(3,3-dimethyl-3,4-dihydroisoquinoline) (I) was synthesized. Its crystal structure was determined by X-ray diffraction analysis. Compound I crystallizes as isomer that is intermediate between the syn- and anti-forms with the angle of rotation between the bicyclic fragments equal to 90.1°. The N(1)=C(1) bond length is 1.276(4) ± 0.003 A. |
Databáze: | OpenAIRE |
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