Preparation of Cellulose Oligomers from Cellulose Triacetate (Standard Procedure)

Autor:	J. Pyplo-Schnieders, Hartmut Redlich, P. Arndt, R. Gerdes, S. Huschens
Rok vydání:	2005
Předmět:	Cellulose triacetate chemistry.chemical_compound Materials science Polymers and Plastics chemistry Polymer chemistry Organic chemistry Pivalic anhydride Cellulose Boron trifluoride Dichloromethane Standard procedure
Zdroj:	Cellulose. 12:317-326
ISSN:	1572-882X 0969-0239
DOI:	10.1007/s10570-004-3387-6
Popis:	This communication reports the detailed procedure for the cleavage of cellulose triacetate (30 g scale) with pivalic anhydride and boron trifluoride etherate in dichloromethane (pivaloylysis). With this mild and efficient method the cellulose oligomers up to the octasaccharide can be obtained in gram scale. Full characteristic data of this compounds are given.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::1f060209038006ee564ccb55bca838bc https://doi.org/10.1007/s10570-004-3387-6 Zobrazit plný text záznamu Full text from SpringerLink