Alkanedisulfamic Acid Functionalized Silica-Coated Magnetic Nanoparticles: Preparation and Catalytic Investigation in Synthesis of Mono-, Bis- and Tris[bis(4-hydroxycoumarinyl)methanes]

Autor: Marzie Karimi, Zeinab Dalirnasab, Zahra Eftekhari, Ali Reza Karimi
Rok vydání: 2014
Předmět:
Zdroj: Synthesis. 46:3180-3184
ISSN: 1437-210X
0039-7881
DOI: 10.1055/s-0034-1378667
Popis: Alkanedisulfamic acid-functionalized silica-coated magnetic nanoparticles (ADSA-MNPs) were prepared by a simple method and evaluated as efficient catalysts for the preparation of mono-, bis-, and tris[bis(4-hydroxycoumarinyl)methanes] through condensation of 4-hydroxy-2H-coumarin-2-one with mono-, di-, or trialdehydes, respectively. The heterogeneous nanocatalyst was readily recovered from the reaction mixture by using external magnet and was reused five times without significant loss of catalytic activity.
Databáze: OpenAIRE