Alkanedisulfamic Acid Functionalized Silica-Coated Magnetic Nanoparticles: Preparation and Catalytic Investigation in Synthesis of Mono-, Bis- and Tris[bis(4-hydroxycoumarinyl)methanes]
Autor: | Marzie Karimi, Zeinab Dalirnasab, Zahra Eftekhari, Ali Reza Karimi |
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Rok vydání: | 2014 |
Předmět: | |
Zdroj: | Synthesis. 46:3180-3184 |
ISSN: | 1437-210X 0039-7881 |
DOI: | 10.1055/s-0034-1378667 |
Popis: | Alkanedisulfamic acid-functionalized silica-coated magnetic nanoparticles (ADSA-MNPs) were prepared by a simple method and evaluated as efficient catalysts for the preparation of mono-, bis-, and tris[bis(4-hydroxycoumarinyl)methanes] through condensation of 4-hydroxy-2H-coumarin-2-one with mono-, di-, or trialdehydes, respectively. The heterogeneous nanocatalyst was readily recovered from the reaction mixture by using external magnet and was reused five times without significant loss of catalytic activity. |
Databáze: | OpenAIRE |
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