Fabrication and evaluation of gold nanoparticles by ball milling, Hall-Williamson and x-ray diffraction method
| Autor: | Purushotham Endla, Veerati Radhika |
|---|---|
| Rok vydání: | 2021 |
| Předmět: |
010302 applied physics
Fabrication Materials science Period (periodic table) Strain (chemistry) Analytical chemistry Nanoparticle 02 engineering and technology 021001 nanoscience & nanotechnology 01 natural sciences Colloidal gold Vacancy defect 0103 physical sciences X-ray crystallography 0210 nano-technology Ball mill |
| Zdroj: | Materials Today: Proceedings. 47:4993-4995 |
| ISSN: | 2214-7853 |
| DOI: | 10.1016/j.matpr.2021.04.451 |
| Popis: | The aim of this paper is to use a high-energy ball mill to convert micro-sized Au powder into nano-structured Au powder; it means Au (Gold) NanoParticles (AuNPs) have been fabricated in this present work. The ball milling process took a total of 20 h to complete. First I have taken initial sample 0 h. after every 4 h of milling time period i.e., 4, 8, 12, 16 and 20 h have been calculated, all the values best fit with the previous researcher values. The HWFM and integrated intensities of Bragg reflections are used to measure strain and B value. In Au, the B value increases as the strain also increases. The B values for zero strain were determined using the relationship between strain and the effective B value. The energy of vacancy formation as a function of strain has been investigated. |
| Databáze: | OpenAIRE |
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