A Convenient Large Scale Synthesis of O-Benzylhydroxylamine

Autor: Raffaello Giorgi, Bonaccorsi Fabrizio
Rok vydání: 1997
Předmět:
Zdroj: Synthetic Communications. 27:1143-1147
ISSN: 1532-2432
0039-7911
DOI: 10.1080/00397919708003349
Popis: Synthetically useful O-benzylhydroxylamine can be conveniently prepared in large scale by reaction of N-hydroxyphthalimide and benzyl chloride in phase transfer conditions, followed by acidic hydrolysis of N-benzyloxyphthalimide. The overall yield is over 65%.
Databáze: OpenAIRE