A Convenient Large Scale Synthesis of O-Benzylhydroxylamine
Autor: | Raffaello Giorgi, Bonaccorsi Fabrizio |
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Rok vydání: | 1997 |
Předmět: | |
Zdroj: | Synthetic Communications. 27:1143-1147 |
ISSN: | 1532-2432 0039-7911 |
DOI: | 10.1080/00397919708003349 |
Popis: | Synthetically useful O-benzylhydroxylamine can be conveniently prepared in large scale by reaction of N-hydroxyphthalimide and benzyl chloride in phase transfer conditions, followed by acidic hydrolysis of N-benzyloxyphthalimide. The overall yield is over 65%. |
Databáze: | OpenAIRE |
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