Quantitative Analysis of Zirconium Oxide by Direct Current Glow Discharge Mass Spectrometry Using a Secondary Cathode

Autor:	R. Van Grieken, Wim Schelles
Rok vydání:	1997
Předmět:	Reproducibility Glow discharge Glow Discharge Mass Spectrometry Chemistry Direct current Analytical chemistry Mass spectrometry Cathode Analytical Chemistry law.invention Impurity law Quantitative analysis (chemistry) Spectroscopy
Zdroj:	Journal of Analytical Atomic Spectrometry. 12:49-52
ISSN:	1364-5544 0267-9477
DOI:	10.1039/a605397a
Popis:	A dc GD mass spectrometer has been used for the analysis of ZrO 2 samples with known amounts of artificial impurities. For this purpose the secondary cathode technique has been used. The research work focused both on the methodological aspects of the atomization of the ZrO 2 and on some quantitative aspects, with direct analytical interest. The reproducibility was found to be better than 10% RSD in most cases; the accuracy of the ‘standardless’, raw results was within a factor of 2–3 of the known concentration.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::1b29d5f66e6ff90944a8f7c54687733b https://doi.org/10.1039/a605397a Zobrazit plný text záznamu