Convenient synthesis of deuterated aluminium hydrides

Autor:	Claudia Weidenthaler, Michael Felderhoff, Roland H. Pawelke, Ferdi Schüth
Rok vydání:	2008
Předmět:	Diffraction Materials science Mechanical Engineering Inorganic chemistry Metals and Alloys chemistry.chemical_element Condensed Matter Physics Alkali metal Hydrogen storage Deuterium chemistry Mechanics of Materials Aluminium General Materials Science Lithium Ball mill
Zdroj:	Scripta Materialia. 59:515-517
ISSN:	1359-6462
DOI:	10.1016/j.scriptamat.2008.04.042
Popis:	We describe the ball-milling synthesis of alkali metal deuterides from commercial lithium aluminium deuteride. This reaction principle was exemplified by the mechanochemical synthesis of NaAlD 4 and KAlD 4 . NaAlD 4 was prepared on the multi-gram scale by this procedure and purified by standard wet-chemical separation. Pure NaAlD 4 was obtained and used for the synthesis of Ca(AlD 4 ) 2 . The formation of all products was verified by X-ray diffraction.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::18996db62477747feb181ced2028f16f https://doi.org/10.1016/j.scriptamat.2008.04.042 Zobrazit plný text záznamu Full Text from ScienceDirect