Aufreinigung von Fumonisinen und ihren Hydrolysaten über ein neuartiges Festphasenextraktions-Material

Autor: I. Zimmer, Kapp T, H. Klaffke, P. Majerus, R. Weber, Ewald Usleber, Erwin Märtlbauer, R. Tiebach, Stan H-J
Rok vydání: 2002
Předmět:
Zdroj: Mycotoxin Research. 18:113-116
ISSN: 0178-7888
DOI: 10.1007/bf02946076
Popis: Tests with various clean-up materials after optimisation of different parameters showed that the use of Oasis® material resulted in matrixless chromatograms in HPLC-FLD. The selectivity and detection limit of the method was improved by using LC-MS/MS as the detection system. Mean recovery was 100%, and no negative food matrix effects could be observed.
Databáze: OpenAIRE