Aufreinigung von Fumonisinen und ihren Hydrolysaten über ein neuartiges Festphasenextraktions-Material
Autor: | I. Zimmer, Kapp T, H. Klaffke, P. Majerus, R. Weber, Ewald Usleber, Erwin Märtlbauer, R. Tiebach, Stan H-J |
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Rok vydání: | 2002 |
Předmět: | |
Zdroj: | Mycotoxin Research. 18:113-116 |
ISSN: | 0178-7888 |
DOI: | 10.1007/bf02946076 |
Popis: | Tests with various clean-up materials after optimisation of different parameters showed that the use of Oasis® material resulted in matrixless chromatograms in HPLC-FLD. The selectivity and detection limit of the method was improved by using LC-MS/MS as the detection system. Mean recovery was 100%, and no negative food matrix effects could be observed. |
Databáze: | OpenAIRE |
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