Preparation of 2,3,3,3-tetrafluoropropene from trifluoroacetylacetone and sulphur tetrafluoride

Autor:	Michael G. Barlow, M. Nickkho-Amiry, R. Eric Banks
Rok vydání:	1997
Předmět:	Olefin fiber Organic Chemistry Inorganic chemistry Infrared spectroscopy Hydrogen fluoride Biochemistry Spectral line Inorganic Chemistry chemistry.chemical_compound chemistry 2 3 3 3-Tetrafluoropropene Yield (chemistry) Environmental Chemistry Sulphur tetrafluoride Physical and Theoretical Chemistry
Zdroj:	Journal of Fluorine Chemistry. 82:171-174
ISSN:	0022-1139
Popis:	Practical details are presented for the laboratory preparation of 2,3,3,3-tetrafluoropropene in good yield from trifluoroacetylacetone and sulphur tetrafluoride in the presence of hydrogen fluoride. The gas-phase IR spectrum of the tetrafluoropropene (b.p., −28 °C) is reproduced and a detailed analysis of the olefin's nuclear magnetic resonance (NMR) spectra (1H, 13C, 19F) is provided.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::152d88d534eae65f55ba15a6fcf4d064 https://doi.org/10.1016/s0022-1139(96)03556-7 Zobrazit plný text záznamu Full Text from ScienceDirect