Response Surface Optimization of Multilayer Graphene Growth on Alumina-Supported Bimetallic Cobalt–Nickel Substrate
Autor: | Soraya Hosseini, Suraya Abdul Rashid, Mohd Nizar Hamidon, Ismayadi Ismail, Bamidele Victor Ayodele, May Ali Alsaffar, Faizah Md Yasin, Farahnaz Eghbali Babadi |
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Rok vydání: | 2020 |
Předmět: |
Multidisciplinary
Materials science Central composite design Graphene 010102 general mathematics Substrate (chemistry) Chemical vapor deposition 01 natural sciences law.invention Volumetric flow rate symbols.namesake Crystallinity Chemical engineering law symbols Response surface methodology 0101 mathematics Raman spectroscopy |
Zdroj: | Arabian Journal for Science and Engineering. 45:7455-7465 |
ISSN: | 2191-4281 2193-567X |
DOI: | 10.1007/s13369-020-04586-4 |
Popis: | This study investigates the optimization of multilayer graphene (MLG) growth on Co–Ni/Al2O3 substrate. The MLG synthesized by chemical vapor deposition technique (CVD) was characterized using various instrument techniques. The surface area and pore volume of the MLG were estimated as ~ 642 m2/g and ~ 2.7 cm3/g, respectively. The Raman spectrometric analysis showed evidence of MLG. The effects of parameters such as temperature, Co–Ni composition and ethanol flow rate were investigated using response surface methodology (RSM) and central composite design. The maximum MLG yield of 77% was attained at optimum conditions of 800 °C, Co–Ni composition of 0.3/0.7 and ethanol flow rate of 11 ml/min. The analysis of variance (ANOVA) results showed that the RSM quadratic model is significant with a p value |
Databáze: | OpenAIRE |
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