Convenient, Microwave-Assisted, One-Pot Synthesis of Photochromic Fulgimides Bearing Reactive Groups

Autor: Xiaoliu Li, Shichong Pang, Pingzhu Zhang, Hua Chen, Cuiying Li
Rok vydání: 2009
Předmět:
Zdroj: Synthetic Communications. 40:157-166
ISSN: 1532-2432
0039-7911
DOI: 10.1080/00397910902964809
Popis: A convenient, microwave-assisted, one-pot synthesis of the fulgimides (3) bearing reactive groups on N-substituents from the corresponding fulgides (1a–d) and amines (2a–e) is described. The synthesis provided the functionalized fulgimides (3) in yields of 50–84% under microwave irradiation within 25 min in the presence of 4-dimethylaminopyridine (DMAP) and dicyclohexylcarbodiimide (DCC).
Databáze: OpenAIRE