Fibril formation through self-assembly of a simple glycine derivative and X-ray diffraction study
| Autor: | Suvendu Maity, Prasanta Ghosh, Arpita Dutta, Purak Das, Suven Das |
|---|---|
| Rok vydání: | 2020 |
| Předmět: |
02 engineering and technology
010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences 0104 chemical sciences Inorganic Chemistry chemistry.chemical_compound Crystallography Fibril formation chemistry Simple (abstract algebra) Glycine X-ray crystallography General Materials Science Self-assembly 0210 nano-technology Derivative (chemistry) |
| Zdroj: | Zeitschrift für Kristallographie - Crystalline Materials. 235:47-51 |
| ISSN: | 2196-7105 2194-4946 |
| DOI: | 10.1515/zkri-2019-0062 |
| Popis: | N-(N-benzoyl glycinyl)-N,N′-dicyclohexylurea was synthesised by conjugating N-benzoyl glycine and dicyclohexylcarbodiimide (DCC) using triethylamine as base catalyst. A single crystal X-ray diffraction study reveals that the compound self-assembles into a supramolecular sheet structure by intermolecular N–H · · · O, C–H · · · O hydrogen bonding and non-bonding van der Waals interactions. A high resolution transmission electronic microscopic (HR-TEM) image of the compound exhibits formation of fibrils in the solid state. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|