A continuous flow investigation of sulfonyl chloride synthesis using N-chloroamides: optimization, kinetics and mechanism
Autor: | Dominik Polterauer, Dominique M. Roberge, Paul Hanselmann, Ryan Littich, Christopher A. Hone, C. Oliver Kappe |
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Rok vydání: | 2022 |
Předmět: | |
Zdroj: | Reaction Chemistry & Engineering. 7:2582-2592 |
ISSN: | 2058-9883 |
DOI: | 10.1039/d2re00280a |
Popis: | We develop a continuous flow protocol for the synthesis of sulfonyl chlorides from disulfides and thiols, using 1,3-dichloro-5,5-dimethylhydantoin (DCH) as a dual-function reagent for oxidative chlorination. |
Databáze: | OpenAIRE |
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