Direct-Deposition Infrared Spectrometry with Gas and Supercritical Fluid Chromatography
Autor: | Elizabeth. Shafter, Steven M. Pyle, Donald F. Gurka, Richard Titus |
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Rok vydání: | 1994 |
Předmět: | |
Zdroj: | Analytical Chemistry. 66:2521-2528 |
ISSN: | 1520-6882 0003-2700 |
DOI: | 10.1021/ac00087a017 |
Popis: | A direct-deposition Fourier transform infrared (FT-IR) system has been evaluated for applicability to gas chromatography (GC) and supercritical fluid chromatography (SFC) of environmental analytes. A 100-μm i.d. fused-silica transfer line was used for GC, and a 50-μm transfer line with an integral restrictor was used for SFC. Minimum identifiable quantities for GC/FT-IR ranged from 0.5 to 2.0 ng. This is over an order of magnitude better than those reported for light-pipe FT-IR by this laboratory |
Databáze: | OpenAIRE |
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