Autor: |
H. Hunziker, Hs.H. Günthard, R. Meyer, W. E. Good |
Rok vydání: |
1962 |
Předmět: |
|
Zdroj: |
Helvetica Chimica Acta. 45:59-62 |
ISSN: |
0018-019X |
Popis: |
Pure acetone-d6 has been prepared by reaction of heavy water with propyne-d4 in the liquid phase and a mercury catalyst. Propyne-d4 was obtained by hydrolysis of magnesium carbide Mg2C3 with heavy water. A practical procedure for 20 g amounts of acetone-d6 is given in detail. Its over-all consumption of heavy water exceeds the theoretical amount by only 5–10%. |
Databáze: |
OpenAIRE |
Externí odkaz: |
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