Autor: |
Greg Tucker, Prasan Swatsitang, Daniel Jardine, Kevin Robards |
Rok vydání: |
2000 |
Předmět: |
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Zdroj: |
Analytica Chimica Acta. 417:231-240 |
ISSN: |
0003-2670 |
Popis: |
Various methods were compared for the recovery of phenolic compounds from sweet orange. The need for careful consideration of sample preparation was demonstrated. In the case of cinnamic acids, hydroxide-treatment was essential to liberate the bound acids. Ferulic acid was the predominant phenol in alkali-treated extracts. Positive and negative ion electrospray ionisation mass spectra were systematically investigated for a range of phenols. Detection limits were significantly lower in negative ion than in positive ion mode. However, positive ion mode provided additional structural information for many of the compounds. |
Databáze: |
OpenAIRE |
Externí odkaz: |
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