Adhesion and fracture of tantalum nitride films

Autor: D.P. Norwood, S. Venka-taraman, N.R. Mody, J.E. Angelo, Robert Q. Hwang, W.W. Gerberich
Rok vydání: 1998
Předmět:
Zdroj: Acta Materialia. 46:585-597
ISSN: 1359-6454
DOI: 10.1016/s1359-6454(97)00243-7
Popis: Indentation fracture and continuous nanoscratch testing were used in this study to determine the effects of compressive residual stresses on the fracture of thin sputter-deposited tantalum nitride films. Some films were tested in the as-deposited condition while others were vacuum annealed at 300 C. The only discernible change in structure was a surface rearrangement of atoms into parallel arrays of striations on the vacuum annealed samples revealing a high compressive residual stress state after deposition. Comparison of results and application of mechanics-based models showed that these stresses had a strong effect on the fracture of the as-deposited films. The models also provided a good measure of the residual stress levels and interfacial strain energy release rates.
Databáze: OpenAIRE