Preparation and characterization of amorphous nanometre sized Fe3O4powder
Autor: | Aharon Gedanken, Ruslan Prozorov, X. Cao, Israel Felner, G. Katabi, Yu. Koltypin |
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Rok vydání: | 1997 |
Předmět: | |
Zdroj: | Journal of Materials Chemistry. 7:1007-1009 |
ISSN: | 1364-5501 0959-9428 |
DOI: | 10.1039/a606739e |
Popis: | A method for the preparation of amorphous Fe 3 O 4 powder with a particle size of ca. 25 nm is reported. Amorphous Fe 3 O 4 powder can be simply synthesized by slowly exposing amorphous Fe powder to the air. The amorphous properties of Fe 3 O 4 nanoparticles were characterized by X-ray diffraction, Mossbauer spectroscopy, transmission electron micrography, differential scanning calorimetry and quantum design SQUID magnetization measurements. This amorphous Fe 3 O 4 powder is superparamagnetic and its magnetization at room temperature is very low ( |
Databáze: | OpenAIRE |
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