Phase transformations of siderite ore by the thermomagnetic analysis data

Autor: N.O. Dudchenko, A.B. Brik, V.P. Ponomar
Rok vydání: 2017
Předmět:
Zdroj: Journal of Magnetism and Magnetic Materials. 423:373-378
ISSN: 0304-8853
DOI: 10.1016/j.jmmm.2016.09.124
Popis: Thermal decomposition of Bakal siderite ore (that consists of magnesium siderite and ankerite traces) was investigated by thermomagnetic analysis. Thermomagnetic analysis was carried-out using laboratory-built facility that allows automatic registration of sample magnetization with the temperature (heating/cooling rate was 65°/min, maximum temperature 650 °C) at low- and high-oxygen content. Curie temperature gradually decreases with each next cycles of heating/cooling at low-oxygen content. Curie temperature decrease after 2nd cycle of heating/cooling at high-oxygen content and do not change with next cycles. Final Curie temperature for both modes was ~320 °C. Saturation magnetization of obtained samples increases up to 20 Am2/kg. The final product of phase transformation at both modes was magnesioferrite. It was shown that intermediate phase of thermal decomposition of Bakal siderite ore was magnesiowustite.
Databáze: OpenAIRE