Determination of methylbenzo[a]pyrene isomers in a coal tar standard reference material using liquid chromatography and Shpol'skii spectrometry
Autor: | Stephen A. Wise, J. Bellocq, Philippe Garrigues |
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Rok vydání: | 1990 |
Předmět: | |
Zdroj: | Fresenius' Journal of Analytical Chemistry. 336:106-110 |
ISSN: | 1618-2650 0937-0633 |
DOI: | 10.1007/bf00322546 |
Popis: | Concentrations of individual methylbenzo[a]pyrene (MBP) isomers were determined in a coal tar standard reference material (SRM 1597) by using liquid chromatography (LC) (normal- and reversed-phase) and high resolution Shpol'skii spectrometry (HRS) at 15 K. This is the first report on the unambiguous identification and quantification of each MBP isomer in a real sample, and this report contains information on the distribution of these highly carcinogenic compounds in coal tar. |
Databáze: | OpenAIRE |
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