Comparison of Different Methods for Extraction from Lavender: Yield and Chemical Composition
Autor: | Katarína Čížová, Andrea Škulcová, Aleš Ház, Alexandra Sládková, Michal Jablonský, Helena Ramajová |
---|---|
Rok vydání: | 2016 |
Předmět: |
Chromatography
Mechanical Engineering Butanol 010401 analytical chemistry Extraction (chemistry) 02 engineering and technology 021001 nanoscience & nanotechnology 01 natural sciences 0104 chemical sciences law.invention Steam distillation Solvent chemistry.chemical_compound Eucalyptol chemistry Linalool Mechanics of Materials law General Materials Science 0210 nano-technology Protic solvent Dichloromethane |
Zdroj: | Key Engineering Materials. 688:31-37 |
ISSN: | 1662-9795 |
DOI: | 10.4028/www.scientific.net/kem.688.31 |
Popis: | A comparative study of accelerated solvent extraction (ASE) with two conventional volatile isolation methods including traditional steam distillation and Soxhlet extraction was performed on lavender. ASE was carried out by butanol (polar protic solvent) or dichloromethane (nonpolar solvent) and the temperature was 120°C. Separation and identification of the components was carried out by GC/MS. The main components of the analysed samples were Linalool (14.79%), α-Terpineol (4.42%), Linalool oxide (furanoid) (2.92%), cis-linalyl oxide (2.8%), α-Bisabolol (1.86%) and Octacosane (1.56%) for steam distillation; for ASE (dichlormethane): β-Terpineol (2.06%), Linalyl anthranilate (1.82%), Largeracetal (1.82%), Eucalyptol (1.74%), Linalool (1.73%), Coumarine (1.28%) and Caryophylene oxide (1.08%); for ASE (butanol): Lageracetal (8.29%), Octacosane (1.75%), Eucalyptol (1.05%) and Caryophyllene oxide (1.02%) and for Soxhlet (butanol): Largeracetal (11.42%), Linalool (3.36%), Coumarine (0.83%) and Eucalyptol (0.74%). The study has shown that ASE is a fast and environmentally sustainable technique, using butanol and dichloromethane as solvent for the extraction of extractive compounds from lavender. |
Databáze: | OpenAIRE |
Externí odkaz: |