A new triclinic polymorph of 4,5,6-trimethyl-1-phenyl-3,4-dihydropyrimidine-2(1H)-thione

Autor: Eliyanti A. Othman, Bohari Mohd. Yamin, Nur Liyana Ismail
Rok vydání: 2007
Předmět:
Zdroj: Acta Crystallographica Section E Structure Reports Online. 63:o2442-o2443
ISSN: 1600-5368
DOI: 10.1107/s1600536807016844
Popis: The title crystal structure, C13H16N2S, is a triclinic polymorph of the previously reported ortho­rhom­bic structure [Yamin, Kasim & Hamzah (2005). Acta Cryst. E61, o55–o57]. In both structures, the phenyl group is almost perpendicular to the pyrimidine-2-thione ring. In the triclinic structure, inversion-related molecules are linked to form a dimer by N—H⋯S hydrogen bonds, whereas in the ortho­rhom­bic polymorph two independent mol­ecules are linked by N—H⋯S hydrogen bonds to form a dimer.
Databáze: OpenAIRE