Synthesis of nanocrystalline Fe13at.%B7at.%Si by mechanical alloying

Autor:	Benlih Huang, Enrique J. Lavernia, Adel A. Sharif, Paula J. Crawford, R.J. Perez
Rok vydání:	1995
Předmět:	Diffraction Materials science Scattering Mechanical Engineering Metallurgy Analytical chemistry Condensed Matter Physics Spectral line Nanocrystalline material Lattice constant Mechanics of Materials Lattice (order) General Materials Science Dissolution
Zdroj:	Materials Science and Engineering: A. 204:217-221
ISSN:	0921-5093
Popis:	The synthesis of nanocrystalline Fe-13at.%B-7at.%Si using mechanical alloying of elemental powders in a SPEX mill was investigated. Precise lattice parameter measurements provide insight into the dissolution of Si and B in the nanocrystalline Fe lattice. These data indicate that the complete dissolution of Si in the crystalline Fe matrix required 128 h milling. Only 35% of the total B content was estimated to be in solution after 128 h. Debris from vial and ball wear after this extended milling, however, is found to represent over 35 wt.% of the final composition, and to produce an increase in lattice parameter of approximately 3.7 × 10 −7 nm per hour of milling. In addition, the present results indicate that the disappearance of Si peaks in the X-ray diffraction spectra may be related more directly to the low atomic scattering factor of Si than to its dissolution in Fe.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::0029740dd29948825182e8235177fadd https://doi.org/10.1016/0921-5093(95)09964-6 Zobrazit plný text záznamu Full Text from ScienceDirect