Effect of acid modification on physicochemical characteristics of Kpautagi clay

Autor: Matthew A. ONU, Joseph O. OKAFOR, Abdusalami S. KOVO, Yahaya S. MOHAMMAD
Jazyk: angličtina
Rok vydání: 2016
Předmět:
Zdroj: Leonardo Journal of Sciences, Vol 15, Iss 28, Pp 87-94 (2016)
ISSN: 1583-0233
Popis: Chemical activation was carried out on the kaolin clay obtained from Kpautagi Area in Niger State using sulfuric and hydrochloric acids. In order to study the effect of acid activation, the physicochemical characteristics of the Kpautagi clay were determined before and after acid modification and the results obtained were subsequently compared. These characteristics include surface morphology, surface functional groups, surface area and pore volume. Characterization results showed that acid modification of Kpautagi kaolin clay with sulphuric and hydrochloric acids improved the surface area of the clay from 7.598m2/g to 15.5cm2/g and 13.2cm2/g respectively and enhancement in pore volume and average pore diameter were also noted. The changes in the characteristics of the clay after acid modification were further supported by the Scanning Electron Microscope (SEM) micrographs and Fourier Transformed Infrared Spectroscope (FTIR) spectra. Therefore, the outcome of this study shows that sulphuric and hydrochloric acid could be used to improve the characteristics of Kpautagi clay but better performance could be achieved employing sulphuric acid.
Databáze: OpenAIRE