Controlled Stepwise Synthesis and Characterization of a Ternary Multicomponent Crystal with 2-Methylresorcinol

Autor:	Komisarek, Daniel (M. Sc.), Schauerte, Carsten (Dr. rer. nat.), Merz, Klaus (Dr. rer. nat.)
Jazyk:	angličtina
Rok vydání:	2020
Předmět:	ddc:540 cocrystallization mechanism multicomponent cocrystal cocrystal synthesis
Zdroj:	Chemistry Volume 2 Issue 1 Pages 9-100
ISSN:	2624-8549
DOI:	10.3390/chemistry2010009
Popis:	A typical approach of a multicomponent crystal design starts with a retrosynthetic analysis of the target molecule followed by a one-pot reaction of all components. To develop protocols for multicomponent crystal syntheses, controlled stepwise syntheses of a selected crystalline ternary multicomponent system \(\bf 1\) involving 2-methylresorcinol (MRS), tetramethyl-pyrazine (TMP), and 1,2-bis(4-pyridyl)ethane (BPE) are presented. The obtained binary cocrystals \(\bf 2\) (involving MRS and TMP) and \(\bf 3\) (involving MRS and BPE) as well as the final resulting ternary multicomponent system \(\bf 1\) were characterized by X-ray analysis.
Databáze:	OpenAIRE
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