Microstructure and interphase magnetic coupling in Nd2Fe14B/alpha-Fe nanocomposites obtained by mechanical milling and short time annealing

Autor: Mican, Sever, Hirian, Răzvan, Diop, Leopold, Chicinaş, Ionel, Isnard, Olivier, Pop, Viorel
Přispěvatelé: Babes-Bolyai University [Cluj-Napoca] (UBB), Matériaux, Rayonnements, Structure (MRS), Institut Néel (NEEL), Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Centre National de la Recherche Scientifique (CNRS)-Université Grenoble Alpes [2016-2019] (UGA [2016-2019])-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Centre National de la Recherche Scientifique (CNRS)-Université Grenoble Alpes [2016-2019] (UGA [2016-2019]), Universitatea Tehnica din Cluj-Napoca (UTCN), Michetti, Armelle
Jazyk: angličtina
Rok vydání: 2016
Předmět:
Zdroj: Romanian Journal of Physics
Romanian Journal of Physics, 2016, 61 (3-4), pp.506-517
Popis: International audience; The effects of short time annealing and soft phase pre-milling on the structural and magnetic properties of 6 h milled Nd2Fe14B/10wt% Fe magnetic nanocomposites were investigated. The X-ray diffraction peaks of Nd2Fe14B disappeared after milling due to crystal structure damage, this effect being more pronounced when using pre-milled Fe. After annealing, the characteristic peaks of Nd2Fe14B were restored with a limited growth of the α-Fe crystallites. The best exchange coupling was obtained for the samples which contain unmilled Fe as the soft phase. The maximum coercive field is 0.61 T. The samples containing pre-milled Fe have lower coercive field values, but show a higher remanence. The Nd2Fe14B/α-Fe exchange coupling is analysed.
Databáze: OpenAIRE