Titrimetric and Polarographic Determination of Carminic Acid and its Quantification in Cochineal (Dactylopius coccus) Extracts

Autor: Octavio Reyes-Salas, Marcos Juárez-Espino, José Manzanilla-Cano, Manuel Barceló-Quintal, Adela Reyes-Salas, Reyna Rendón-Osorio
Jazyk: angličtina
Rok vydání: 2011
Předmět:
Zdroj: Universidad Nacional Autónoma de México
UNAM
Redalyc-UNAM
Journal of the Mexican Chemical Society (México) Num.2 Vol.55
Universidad Autónoma de Yucatán
UAY
Redalyc-UAY
Popis: "The purity of synthetic carminic acid was quantified using potentiometric and conductimetric titrations, allowing its use as a secondary standard because there is not a primary one. Polarographic analysis (in ethanol-water 50:50, v/v) of carminic acid showed two reduction signals, each with a different number of electrons. The first reduction had more Nernstian behaviour and can be applied in analyses. Differential pulse polarography (DPP) produced a detection limit of 0.55 ¿g mL-1. The results indicate that DPP can be used to determine carminic acid content in cochineal extracts."
Databáze: OpenAIRE