Autor: |
Falck, J. R., Anjaiah, Siddam, Raju Tuniki, Venugopal, Raj Gopal, V., Capdevila, Jorge H. |
Zdroj: |
Journal of Labelled Compounds and Radiopharmaceuticals; March 2006, Vol. 49 Issue: 3 p245-252, 8p |
Abstrakt: |
Deuterated arachidonic acid and 20‐HETE were prepared in good overall yields and high stereoselectivities. Key transformations include a trans‐specific vinyl dibromide reduction and Suzuki cross‐couplings to a lithium borate or a 9‐BBN borane. These standards are three and two mass units higher, respectively, than their naturally occurring counterparts and are useful in mass spectrometry analysis. Copyright © 2006 John Wiley & Sons, Ltd. |
Databáze: |
Supplemental Index |
Externí odkaz: |
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