Autor: |
Khusainova, Narkis G., Mostovaya, Olga A., Azancheev, Nail M., Litvinov, Igor A., Krivolapov, Dmitry B., Cherkasov, Rafael A. |
Zdroj: |
Mendeleev Communications; September 2004, Vol. 014 Issue: 5 p212-214, 3p |
Abstrakt: |
The reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with (rac)-butane-2,3-diol at temperatures below 0 C leads to the formation of a hydrospirophosphorane containing both a diazaphospholene and a dioxaphospholane ring system and a β-hydroxyalkoxy-1,2,3-diazaphospholene. On heating, these products form a hydrospirotetraoxaphosphorane, its tautomeric monocyclic β-hydroxyalkylphosphite and N-acetyl-N'-isopropylidene-hydrazine. |
Databáze: |
Supplemental Index |
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