| Autor: |
Uechi, Tetsuo, Tsuge, Otohiko, Okita, Shigeru, Kanemasa, Shuji |
| Zdroj: |
Bulletin of the Chemical Society of Japan; October 1983, Vol. 56 Issue: 10 p2922-2926, 5p |
| Abstrakt: |
The title compound crystallizes in the triclinic space group P\bar1 with two fomrula units in a unit cell of dimensions; a=11.621(3), b=15.177(3), c=10.229(2) Å, α=95.63(2), β=105.46(2), and γ=76.43(2)°. The crystal structure was solved by a conventional heavy-atom method and refined by block-diagonal least-squares procedures to give a final Rvalue of 0.050 for 3428 reflections, with Fo>2σ(Fo), collected on a four-circle diffractometer. The bond distance shared between the acenaphthene and the cyclopentane rings is unusually long at 1.596(6) Å, which may result from the additional strain induced by the fusion of these rings. The solvent molecules are disordered in the channel composed of the main molecules. |
| Databáze: |
Supplemental Index |
| Externí odkaz: |
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