| Autor: |
Matmin, Juan, Yuliati, Leny, Shamsuddin, Mustaffa, Lintang, Hendrik Oktendy |
| Zdroj: |
Advanced Materials Research; April 2014, Vol. 925 Issue: 1 p228-232, 5p |
| Abstrakt: |
Herein we report the first example of benzene-1,3,5-tricarboxamide bearing hydrophobic aminododecane side chains (1) which spontaneously forms supramolecular network by a hydrogen bonding interaction. The compound 1 was synthesized by Schotten-Baumann reaction of 1,3,5-benzenetricarbonyl trichloride and 1-aminododecane in the presence of N,N-diisopropylethylamine. Nuclear Magnetic Resonance (NMR), Mass Spectrometry (MS), and Fourier Transform Infrared (FTIR) spectroscopies have proved the successful synthesis of 1 in 93% as white powder solid. The supramolecular organization was successfully utilized for sensing of nitrate anions by deformation of the hydrogen bonding to form inactive nitroso groups. |
| Databáze: |
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