| Autor: |
Crouch, Dennis J., Moran, Donald M., Finkle, Bryan S., Peat, Michael A. |
| Zdroj: |
Journal of Analytical Toxicology; March 1984, Vol. 8 Issue: 2 p63-63, 1p |
| Abstrakt: |
A versatile method for the quantitation of emetine and cephaeline in biological samples is described. Two milliliters of samples containing N-propylprocainamide as the internal standard are buffered to pH 9 and extracted with n-butyl chloride. After subsequent back extraction into 0.01M hydrochloric acid, a portion of the acid layer is analyzed by reversed-phase high performance liquid chromatography with fluorescence detection. Routinely, the minimum level of detection for both drugs is 5 ng/mL and linearity is demonstrated from 5 to 2500 ng/mL. |
| Databáze: |
Supplemental Index |
| Externí odkaz: |
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