Pressurized fluid extraction of essential oil from Lavandula hybridausing a modified supercritical fluid extractor and a central composite design for optimization

Autor: Kamali, Hossein, Jalilvand, Mohammad Reza, Aminimoghadamfarouj, Noushin
Zdroj: Journal of Separation Science (JSS) (formerly Journal of High Resolution Chromatography); June 2012, Vol. 35 Issue: 12 p1479-1485, 7p
Abstrakt: Essential oil components were extracted from lavandin (Lavandula hybrida) flowers using pressurized fluid extraction. A central composite design was used to optimize the effective extraction variables. The chemical composition of extracted samples was analyzed by a gas chromatograph‐flame ionization detector column. For achieving 100% extraction yield, the temperature, pressure, extraction time, and the solvent flow rate were adjusted at 90.6°C, 63 bar, 30.4 min, and 0.2 mL/min, respectively. The results showed that pressurized fluid extraction is a practical technique for separation of constituents such as 1,8‐cineole (8.1%), linalool (34.1%), linalyl acetate (30.5%), and camphor (7.3%) from lavandin to be applied in the food, fragrance, pharmaceutical, and natural biocides industries.
Databáze: Supplemental Index